ANALYTICAL STUDIES OF CU(II),NI(II) AND PD(II) COMPLEX WITH 3- PHENYL-QUINAZOLIN-4(3H)-ONE-2-CARBOXALDEHYDOXIME
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Abstract
3-Phenyl quinazolin-4-(3H)-one-2-carboxaldehydoxime forms water insoluble chelates with Cu(II), Ni(II) and Pd(II). It has been found to be a selective reagent for the gravimetric estimation of these metal ions in presence of many interfering ions. All the che lates have 1:2 (metal: ligand) stoichiometry as shown by Job's method of continuous variation and elemental analysis. Structures of the metal chelates have been established on the basis of magnetic measurements, visible and IR spectra.
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